Standard Reference Gases: Products and Services
Purchases of GML reference gas preparation and calibration services can only be
initiated through a project contract.
Here is an example
Memorandum of Understanding [MOU] contract.
Prices for the services are listed in the MOU.
For more information on calibration services, contact refgas@noaa.gov
- Your project MOU can be obtained by contacting our standards coordinator at refgas@noaa.gov
- No alteration of MOU text please; terms are non-negotiable.
- MOU stipulates payment terms of "Net 30 days after invoice".
- MOU includes a statement of requested materials, shipping and contact information.
- Total cost for each standard includes a cost from each of the following sections, 'Filling of Compressed Gas Cylinders' 'Calibrations of Compressed Gas Cylinders' 'Shipping and Handling'
Purchase and Filling of Compressed Gas Cylinders
The cost of a standard varies with the cylinder type and level of complexity. Cylinders are filled with natural air from Niwot Ridge, Colorado.
- CO2 can be adjusted and calibrated between 250 and 3000 μmol/mol. The target CO2 value is usually within 5 μmol/mol for near ambient concentrations.
- CH4, CO and N2O can be adjusted but with greater targeting variability.
- Cylinder valve connection is CGA-590.
- A standard gas cylinder requires ~6-10 weeks to fill and ~6-10 weeks for each trace gas species to calibrate. Isotopic analyses require ~12 wks per isotope. The normal turn-around time varies due to seasonal logistics and calibration queue.
Cylinder Types
Different types of cylinders are used depending on the molecule of interest.
- Cylinders for CO2/CH4/CO/N2O/SF6 are bare aluminum N30, N60, N80, N150, N265 Luxfer (or equivalent) cylinders. The most common size we use is N150, 29.5 liter internal volume, pressurized to 130 bar, containing approximately 4000 liters of air. Cylinder valves are Ceodeux, brass packless, CGA590 port connection.
- The majority of halocompound standards are prepared in Aculife-treated aluminum cylinders (size AL-150).
Calibrations of Compressed Gas Cylinders
NOAA GML is the World Meteorological Organization (WMO), Global Atmosphere Watch (GAW) Central Calibration Laboratory (CCL) for CO2, CH4, N2O, SF6, and CO. Calibrations results for these species are on official WMO scales. Calibrations for other gases are on internal NOAA scales.
Calibrations can be performed on the stable isotopes of CO2 (13C and 18O) and CH4 (13C). The CO2 stable isotope calibration is based on a provisional scale maintained by INSTAAR at the University of Colorado. Values given for the stable isotopes of CO2 are informational values only.
One recalibration (CO2, CH4, CO, N2O and/or SF6) is included in the cost of the standard. This is highly recommended every 3 years for precision work and should at least be performed at the end of the cylinder's use (20 atm pressure).
Pre-purchase Quotes
For more information and pre-purchase quotes, e-mail refgas@noaa.gov. A quote is necessary before accepting a purchase order. Inquiries can also be made through the following address:
National Oceanic and Atmospheric Administration
Global Monitoring Laboratory
R/GML
325 Broadway
Boulder, CO. 80305
E-Mail refgas@noaa.gov